China: 3D Printing in Glass at the Macro Scale with Micro Resolution

Researchers are mixing up the macro- and the micro- in their latest study, designed to expand the limits of 3D printing with glass. In ‘Three-dimensional laser printing of macroscale glass objects at a micro-scale resolution,’ the authors explain how they created macro-scale 3D objects in glass at a micro-scale resolution—hoping for success which has so far never been attained in two decades of research and effort in femtosecond laser induced chemical etching (FLICE).

The researchers were able to 3D print macro-scale glass objects at heights up to ~3.8 cm with a well-balanced (i.e., lateral vs longitudinal) spatial resolution of ~20 μm:

“The remarkable accomplishment is achieved by revealing an unexplored regime in the interaction of ultrafast laser pulses with fused silica which results in aberration free focusing of the laser pulses deeply inside fused silica,” state the researchers.

They began by ‘loosely focusing’ laser pulses into the silica, etching multiple lines organized into two different grids for both X and Y directions.

The fabrication resolution offered by loosely focusing the picosecond laser pulses into fused
silica. (a) Schematic illustration of inscribing lines within a cube of fused silica along X and Y
direction. Cross-sectional optical micrographs of the lines written along (b) Y and (c) X directions.
(d) Cross-sectional micrographs of the hollow channels produced by chemically etching the
inscribed sample in the last column of (c). Scale bar: 25 m.

The research team noted that their cross section of lines showed an almost completely circular shape. The lines were insensitive to all the following: scan speed, focal position depth, laser writing direction.

“The difference is that with an increasing scan speed, the color in the cross section captured under the microscope in a reflective mode becomes lighter, indicating that a weaker modification of fused silica will be generated with the decrease of the irradiation dose at the increasing scan speed,” explained the authors.

After eliminating nanogratings in the fused silica, they could 3D print with worrying about polarizing the writing laser beam ‘in real time.’ The authors states that this allowed them to simply beam steering in the printing system, making the entire process easier and ‘more robust.’

In the images below, you can get a better understanding of the successes in their work as the authors created the Einstein head with all his ‘fine features’ visible—even the eyelids.

“It proves that the entire sculpture is printed with a decent fabrication resolution from top to the bottom,” said the authors.

The statue of Confucius is extremely detailed also, with an impressively smooth appearance, although this could be further improved with post annealing or laser polishing.

The air turbine includes moveable parts that were printed in the glass, eliminating any need for assembly, and illustrated below.

A laser printed sculpture of Albert Einstein’s head in fused silica. (a) The model and the (b)
front, (c) right, (d) back, and (e) left sides of the sculpture. (f) and (g) are the zoom-in images of (b)
and (e), respectively, to highlight the fine details on the face. Scale bar: 5 mm.

A laser printed sculpture of Confucius in fused silica. (a) The model and the (b) front, (c) left,
(d) back, and (e) right sides of the sculpture. The details of the decorative pattern on the cloth, the
right side of his face, and the left hand hanging behind his body are shown in the insets on the righthand side of the images in (b), (c) and (d), respectively. Scale bar: 5 mm

A laser printed air turbine in fused silica. (a) The whole air turbine model. Inlet and outlet for
air injection are indicated. (b) The interior of the turbine including turbine fan, a driving gear (G3)
and two driven gears (G1 and G2). Each of G1 and G2 is connected with a cam. (c) Digital-camera
captured image of the fabricated turbine. The air direction and the rotation direction of the fan, as
well as the rotation directions of G1, G2 and G3 from a top view are all indicated by the curved
arrows in (c). (d) The initial position of the two cams is pointing to the left as indicated by the two
arrows. (e) Both the cams are rotated in a clockwise direction by 90 as a result of the injected air flow. Scale bar: 5 mm.

“Further improvement on the printing efficiency will be done in the near future by combining a 2D galvo scanner with the 2D motion stage. This design will allow both a high printing speed and a large printing area. The novel 3D glass printing technique is established based on two unconventional characteristics in the interaction of loosely focused picosecond laser pulses with fused silica, namely, the depth-independent aberration-free focusing and the elimination of the self-organized nanograting,” concluded the researchers.

“The physical mechanisms behind these interesting effects have not yet been clarified. We stress that the interaction of ultrafast laser pulses with transparent media under the loose focusing condition is a largely unexplored area of research, which shall inspire significant interest for further investigations. The high-resolution 3D printing of macro-scale objects in glass is expected to have implications in the fields of photonics, microfluidics, and high-precision mechanics.”

The great thing about 3D printing and all the accompanying techniques requiring infinite choices in hardware, software, and materials is that there is always something new to try—and there is always lots to talk about, whether you are a researcher, student, designer, engineer, or one of the many other types of users enthusiastic about 3D design and printing. Fabrication with glass is garnering growing interest, from experimentation with works of art, to metallic glass, to carbohydrate glass. Those are just a few examples, with macro-scale objects taking such studies to a new level of complexity.

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[Source / Images: Three-dimensional laser printing of macroscale glass objects at a micro-scale resolution]

MIT presents the G3DP2 platform – a first for architectural scale 3D printed glass

In 2017, Milan Design Week hosted a set of 3 meter tall glass columns made using 3D printing. The product of the latest fabrication experiment of the Mediated Matter Group at Massachusetts Institute of Technology (MIT) these relatively large structures demonstrated the architectural potential of an ancient material combined with cutting edge technology. Now, in the […]

MIT Researchers Discuss the Evolution of Their Glass 3D Printer

Researchers at MIT were among the first to 3D print glass, creating the G3DP machine a few years ago to create intricate glass structures. Last year, they scaled up the project with G3DP2, a platform that enabled them to 3D print glass on an architectural scale. Now these researchers have documented their work on G3DP2 in a paper entitled “Additive Manufacturing of Transparent Glass Structures.

The researchers had two main goals in the development of G3DP2:

  • Develop an industrial-scale molten glass feedstock 3D printer by extending the research previously conducted at MIT, enhancing the material properties and range of products that could be produced.
  • Develop an architectural-scale 3D-printed glass structure to evaluate the practical capabilities of the new system in an industrial production.

The new platform, they explain, was designed as a two-part vertical assembly: an upper, stationary thermal module with a digitally integrated three-zone heating control system regulating glass flow and a lower, motion module with a four-axis CNC system that moves the print bed.

“In this architecture, the thermal energy applied to the heating system was decoupled from the mechanical load of the motion system,” the researchers state. “This allowed for improved durability of both systems through careful consideration of material properties and detailed analysis of constituent parts supporting each separate module. Still, critical focus was given to the print head itself, situated at the interface between the modules and requiring the highest thermal and mechanical performance from its material choice.”

The researchers describe the upgrades they made that turned G3DP into G3DP2, one of the fastest 3D printers in the world, independent of material. Their objectives were increased speed and scale as well as improved reliability and repeatability, and they achieved all four. Several tests were conducted, beginning with using pens to evaluate motion, then moving on to actual 3D printing. The researchers discuss how to understand and control the behavior of the 3D printed glass, as well as the specifications, engineering and control of the platform.

Once G3DP2 was completed, the researchers used it to 3D print three-meter-tall glass columns for the Lexus “Yet” exhibition at Milan Design Week 2017. The columns consisted of 15 unique 3D printed glass components that were assembled vertically with “thin silicone film joinery and steel post-tensioning systems to ensure vertical stability.” Each column contained a mobile LED light module set on a linear motion system, with the intersection of the moving light rays and the morphology of the glass structures creating a beautiful light show as well as a demonstration of the capabilities of MIT’s 3D glass printer.

“In the future, combining the advantages of this AM technology with the multitude of unique material properties of glass such as transparency, strength, and chemical stability, we may start to see new archetypes of multifunctional building blocks,” the researchers conclude. “Transparent and hollow-section glass tubes simultaneously act as an heating, ventilation, and air conditioning (HVAC) system, performing as structure and vasculatures at the same time at building scale, through which synthetic and biological mediums circulate and react to incoming sunlight and surrounding temperature, passively regulating the building while illuminating the interior space as if they were a dynamic stained glass—embodying the fundamental shift in the notion of glass in architecture from human centric toward a symbiosis between human, inhuman, and the built environment.”

Authors of the paper include Chikara Inamura, Michael Stern, Daniel Lizardo, Peter Houk and Neri Oxman.

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3D Printed Metallic Glass Demonstrates Benefits of Both Metal and Thermoplastics

A team of researchers led by Jan Schroers, Professor of Mechanical Engineering and Materials Science at Yale, has developed a way to 3D print objects from metallic glass. The material is stronger than metal yet has the pliability of plastic, which makes it extremely valuable. The research is published in a paper entitled “3D printing metals like thermoplastics: Fused filament fabrication of metallic glasses.

Extrusion-based 3D printing of metals is still a challenge, but bulk metallic glasses, or BMGs, can undergo continuous softening upon heating, like thermoplastics can. The research team, which also included researchers from Desktop Metal as well as MIT, demonstrated that BMGs can be used to create solid, strong metal components under ambient conditions similar to those in thermoplastic 3D printing.

“It was even surprising to us how practical this process is once we had the processing conditions figured out,” Schroers said.

Metal 3D printing, while gradually becoming more accessible and affordable, is still quite costly, and powder-based 3D printing is prone to flaws and imperfections, which make it even more expensive. The BMG research could save a lot of money and resources for manufacturers, and also eliminate the need to choose between the benefits of thermoplastics and metals.

The researchers worked with a well-characterized and readily available BMG material made from zirconium, titanium, copper, nickel and beryllium. They used amorphous rods one millimeter in diameter and 700 millimeters in length. They used an extrusion temperature of 460°C and an extrusion force of 10 to 1000 Newtons to force the softened fibers through a 0.5 diameter nozzle. A surprise came when they characterized the 3D printed parts.

“We expected high strength in the parallel-to-the-printing orientation, but were very surprised by the strength in the perpendicular orientation,” said Jittisa Ketkaew, a co-author and graduate student in the Schroers lab.

In theory, a wider range of BMGs can also be 3D printed using the researchers’ method.

“We have shown theoretically in this work that we can use a range of other bulk metallic glasses and are working on making the process more practical and commercially usable to make 3D printing of metals as easy and practical as the 3D printing of thermoplastics,” said Schroers.

There is potential for this method to be used in numerous applications, said Punnathat Bordeenithikasem, a co-author and recent Yale graduate who is currently working as a postdoctoral fellow at the NASA Jet Propulsion Laboratory, California Institute of Technology.

“Beyond prototyping, the achievable properties of the printed parts accompanied by the versatility in part design makes this 3D printing technology suitable for fabricating high-performance components for medical, aerospace, and spacecraft applications,” said Bordeenithikasem.

Authors of the paper include Michael A. Gibson, Nicholas M. Mykulowycz, Joseph Shim, Richard Fontana, Peter Schmitt, Andrew Roberts, Jittisa Ketkaew, Ling Shao, Wen Chen, Punnathat Bordeenithikasem, Jonah S. Myerberg, Ric Fulop, Matthew D. Verminksi, Emanuel M. Sachs, Yet-Ming Chiang, Christopher A. Schuh, A. John Hart, and Jan Schroers.

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[Source/Images: Yale]